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INTERNATIONAL JOURNAL OF PHARMACEUTICAL RESEARCH

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Published by : Advanced Scientific Research
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0975-2366
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IJPR 9[3] July - September 2017 Special Issue

July - September 9[3] 2017

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Molecular and Atomic Absorption Spectrophotometric determination of Furosemide via complex formation with Chromium ion

Author: KHITAM JABER NABHAN, ABBAS SHEBEEB HASAN AL-KADUMI, JWAN ODAY ABDULSATTAR
Abstract: Two simple, accurate, precise analytical methods have been proposed for the determination of Furosemide (Fur) including molecular (UV-VIS) and indirect flame atomic absorption spectrophotometry. The method is based on Fur and Cr III complex formation in acid medium. Mole ratio of Fur-Cr complex was (2:1) (L: M). An optimal condition of this study has been estimated (7.0, 70?C, 10minutes, 100µg/ml , benzyl alcohol, 4minutes, 2ml) for pH, temperature, time reaction, concentration of metal ion, extraction organic solvent ,time and volume of extraction for complex formed in molecular spectrophotometry .The optimum parameters for FAAS showed a similarity to molecular (Uv-VIS) except for chromium (?) ion which was 4µg/ml. The analytical data measured were linearity (10-250 µg/ml), (0.5-6 µg/ml), R (0.9987, 0.9972), D.L (2.271-2.903),(0.157-0.174 µg/ml), Recovery % (97.458 - 97.525), (97.212 - 97.330), RSD % (-2.543- -2.475),(-2.788- -2.670) for tablet and injection formulation in molecular(UV-VIS) and FAAS method respectively.
Keyword: Fur, chromium chloride, flame atomic, molecular absorption spectrophotometry, complexation, determination.
DOI: https://doi.org/10.31838/ijpr/2021.13.01.329
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