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INTERNATIONAL JOURNAL OF PHARMACEUTICAL RESEARCH

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IJPR included in UGC-Approved List of Journals - Ref. No. is SL. No. 4812 & J. No. 63703

Published by : Advanced Scientific Research
ISSN
0975-2366
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IJPR 9[3] July - September 2017 Special Issue

July - September 9[3] 2017

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Synthesis and Spectroscopic Studies of some new Metals Complexes With (3 R) -3-hydroxy-2-(3-(4-nitrobenzoyl) thioureido) butanoic acid

Author: TAGHREED ALWAN, BASIMA M. SAHRAN, T. A. HIMDAN
Abstract: 3-(4-hydroxyphenyl)-2-(3-(4-nitrobenzoyl) thioureido) butaanoic acid (HNB) a new ligand was synthesized by reaction of Threonine with (4-Nitrobenzoyl isothiocyanate) by using acetone as a solvent. The prepared ligand (HNB) has been characterized by elemental analysis (CHNS), infrared (FT-IR), electronic spectral (Ultraviolet visible) and(1H,13C-Nuclear Magnetic Resonance) spectra. Some metal ion complexes of (HNB) were prepared and spectroscopic studies by Fourier transform infrared (FTIR), electronic spectral(UV-Vis), molar conductance, magnetic susceptibility and atomic absorption. The results measured showed the formula of six prepared complexes were [M (HNB)2] (M+2 = Manganese, Cobalt, Nickel, Znic, Cadmium and Mercury),from the obtained data tetrahedral structure suggested for all complexes, except Copper complex has a square planer geometry.
Keyword: Threonine, 4-Nitrobenzoyl isothiocyanate
DOI: https://doi.org/10.31838/ijpr/2020.12.03.129
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