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INTERNATIONAL JOURNAL OF PHARMACEUTICAL RESEARCH

A Step Towards Excellence

IJPR included in UGC-Approved List of Journals - Ref. No. is SL. No. 4812 & J. No. 63703

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0975-2366
5 - Years Impact Factor

Year 2012 - 2016

Impact Factor: 1.55

Total Publications: 317

Total Citation: 491

Year 2011 - 2015

Impact Factor: 1.46

Total Publications: 326

Total Citation: 477

Year 2010 - 2014

Impact Factor: 1.3

Total Publications: 313

Total Citation: 407

Year 2009 - 2013

Impact Factor: 0.973

Total Publications: 293

Total Citation: 285

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Spectrophotometric Determination for Bisacodyl Drug by Oxidative Coupling with Ansidine

Author: IQBAL MOHAMMED, ABDULSALAM A. ABDULKAREEM, SUAD T. ALI
Abstract: An efficient, simple, rapid and economical colorimetric method for specific determination of microgram amounts of bisacodyl in pure and pharmaceutical preparations has been developed. The proposed method is based on an oxidative coupling reaction between bisacodyl and ansidine reagent in presence of Sodiumnitroprusside an oxidant agent in neutral media to form an intense purple color product that has a ? max 542.4 nm. Linearity of calibration graph was observed in the range of (1.00–3.00) µg.ml-1 with molar absorptivity of (14.502 ×103 L.mol-1.cm-1) ,a Sandall sensitivity of (0.024 µg.cm-2) , correlation coefficient of (0.990) , detection limit (0.013 µg.ml-1) and the relative standard deviation of RSD% (1.51-5.35).The developed method was applied to successfully for the estimation of bisacodyl tablets and suppositories.
Keyword: Bisacodyl, Determination, Oxidative Coupling, Ansidine
DOI: https://doi.org/10.31838/ijpr/2019.11.03.050
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2017CiteScore
 
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Impact Factor for five years is 1.55 (2012 - 2016)

Year 2011 - 2015 Impact Factor - 1.46 Total Publications - 326 Total Citations - 477